ESI-MS
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Column: ZORBAX Eclips XDB C18 column (3.0 X 250 mm) with a 5-mm particle size (Agilent Technologies)
The mobile phase was 7.5 mM formic acid in MeOH/H2O (20:80, v/v) used at a flow rate of 0.4 mL/min. A 0.3-uLaliquot of sample was injected
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